Presentation Objetives Partners Infrastructures Contact
Nuevas Metodologías Analíticas
para el Estudio y Control
de la Seguridad y Calidad de los Alimentos
1. Available equipment for the scientific program.
The groups involved in the program have at their disposal several instrumental analytical techniques, which represent the most important part of the infrastructure necessary to carry out the program, and which are also available to the rest of the groups involved. These techniques are listed below:

a. Department of Instrumental Analysis and Environmental Chemistry. IQOG. CSIC:
▪ 2 gas chromatographs equipped with a flame ionization detector.
▪ A gas chromatograph coupled to a mass spectrometer.


Cromatógrafo de gases con detector de
espectrometría de masas cuadrupolar.

 

▪ A system for GCxGC comprehensive coupling equipped with a electron capture microdetector.
▪ A gas chromatograph with a electron capture detector.
▪ Pressurized liquid extractor.


b. Dept. of Analytical Chemistry. Faculty of Chemistry. UCM:
▪ A high performance liquid chromatograph-Fl.
▪ An inductively coupled plasma mass Spectrometer.
▪ A gas chromatograph with flame ionization detector.
▪ A liquid Chromatograph with UV detection.
▪ A capillary electrophoresis with UV detection.
▪ A microwave oven.




Horno microondas para extracciones

▪ A focused ultrasound probe.
▪ A system for extraction with molecular imprinted polymers.
▪ A flame atomic absorption spectrometer.
▪ A electrothermal atomization atomic absorption spectrometer.
▪ AF.

c. Dept. of Analytical Chemistry. Faculty of Science. UAH:
▪ 2 systems for capillary electrophoresis with UV diode array detection.
▪ A system for capillary electrophoresis with UV detection.



Equipo de electroforesis capilar

▪ A liquid chromatograph with fluorescence detector.
▪ A liquid chromatograph with diode array UV detection.



Equipo de HPLC-DAD

▪ A liquid chromatograph with UV detection.
▪ A Semi-preparative liquid chromatograph with UV detection with diode array.

d. Faculty of Science. UNED
▪ A high performance liquid chromatograph with fluorescence, conductimetric and UV diode array detection.

e. Group of Thermal Processes in Food Quality and Safety. Instituto del Frio. CSIC:
▪ A high performance liquid chromatograph with UV and refractometric detectors.
▪ A high performance liquid chromatograph with fluorescence detector.
▪ A system for capillary electrophoresis with diode array.
▪ A high performance liquid chromatograph coupled with a mass spectrometer (time shared: 20%).

f. Dept. of Nutrition and Food Science. Faculty of Veterinary Medicine. UCM:
▪An ion-exchange chromatograph with pulsed amperometric detection.

2. Infrastructure acquisition plan
Program funds have been applied in the acquisition of the three instruments described below, that will be used regardless of their location by all the participants when required.

2.1 A comprehensive two dimensional gas chromatography system coupled to a Time of Flight mass spectrometer.
- This equipment was installed at the Institute of General Organic Chemistry (CSIC) and is devoted mainly to the determination of persistent organic pollutants and pesticides from different families, but it may be used in other analytical problems, covering a wide range of applications. It will be used mainly by IQOG groups and by the National University of Distance Education.



Cromatógrafo de gases con detector
de tiempo de vuelo

2.2 A high performance liquid chromatograph coupled to a dual mass spectrometer.
- It is installed in the Department of Analytical Chemistry, Faculty of Chemistry at the UCM. It is primarily used for the analysis of organometallic compounds, acrylamide, proteins, peptides and antibiotics. However, its great potential makes it suitable for a wide range of substances. Will be used by all groups in the program.

2.3 A system for capillary electrophoresis coupled to a mass spectrometer.
This combination is very recent, which suggests that it is still in development and therefore will allow the group of the Dept. of Analytical Chemistry, UAH, the development of the technique. It will be applied to the analysis of amino acids, peptides, proteins, antibiotics, and acrylamide. Their users are, in different extents, all groups in the program, since this technique is quite versatile.

3. Human Resources
The participating groups include, in addition to the research staff, the following technical staff:

Dpt. Instrumental Analysis and Environmental Chemistry:
3 Technicians

Dpt. Analytical chemistry (Chemistry Fac. UCM):

6 Technicians

Technics and Methods in Analytical Chemistry Group (Sciences Fac.. UNED):

1 Technician

Thermal Processes in Food Group (Institute del Frio. CSIC):

1 Technician and 1 Assistant

Fuerthermore, thise contracted or granted staff is available:

Dpt. Instrumental Analysis and Environmental Chemistry:
1 Researcher, 2 postdoctoral granted and 2 Technicians with I3P Contract.

Dpt. Analytical chemistry (Chemistry Fac. UCM):
7 predoctoral granted and 6 technicians

Dpt. Analytical chemistry (Chemistry Fac. UAH):
1 predoctoral contract IV CM PRICT, 3 predocotoral granted UAH, 1 predocotral granted Rep. dominicana-UAH and 1 Technician FINNOVA.

Technics and Methods in Analytical Chemistry Group (Sciences Fac.. UNED):
1 Associated Teacher

Thermal Processes in Food Group (Institute del Frio. CSIC):
2 contracted researchers

Dpt. Nutrition and Bromatology. Veterinary Fac. UCM:
1 postdoctoral granted and 1 predoctoral granted

4. Offer Services
The research groups included in the program have their human resources dedicated to research and teach at the university level. That limits their capacity to provide services for routine analysis to other research groups and industries as other laboratories usually do. Moreover, the potential of knowledge and infrastructure that builds up in the program should be used in their social environment, without detracting its main objectives which are research and teach at CSIC and the University. All these facilities and the results obtained with the program will be screened on the following social sectors:
 
a) The scientific community, through advice and facilities instrumental to other groups that request it and, of course, through the communication of results in journals and scientific conferences.
   
b) The companies, which may establish agreements and contracts to provide different types of analytical services of analytical advice when the company concerned does not have the means to solve their problems. The wide variety of problems associated with the management of quality and safety in the food industry, the enormous volume of legislation and regulations to be met by food suggests that this collaboration could be very useful.
 
c) The Administration, in its various local, regional and national levels. The partnership program with the various agencies responsible for ensuring the purity and quality of food can be very useful on a regular basis and especially when some kind of food scare as unfortunately often happens with some frequency. The program can be a suitable tool and ready to establish and operate appropriate technical measures for immediate resolution of problems.

 
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